Sensitization and intergranular corrosion behavior of high. Strauss test specimens are boiled in a copper sulfate sulfuric acid mixture for 15 hours. Once the specimen has been subjected to the solution boil, it is bent through 180. A detailed study of aisi and stainless steels sss has been conducted to correlate the degree of sensitization dos measured by the.
Astm e426 standard practice for electromagnetic eddy. A26215 standard practices for detecting susceptibility to intergranular attack in austenitic stainless steels corrosion susceptibility copper sulfatesulfuric acid test nitric acid test oxalic acid etch test ferric sulfatesulfuric acid test. The al6xn alloy was designed to be a seawater resistant material and. Astm a262 standard practices for detecting susceptibility to intergranular attack in austenitic stainless steels. The results of astm a262 practice a and practice e bend tests on aged type 316 stainless steel are detailed in table 2. Purchase your copy of astm a262 15 as a pdf download or hard copy directly from the official bsi shop. The first method devised by us exploits the large shortterm difference in weight loss. Astm a262 01 standard practices for detecting susceptibility to. Intergranular corrosion and residual stress determination of a duplex stainless steel pipeline girth weld b gideon1. Corrosion testing techniques and evaluation practices used. United states provided by ihs under license with astm 1 sold to. Determination of susceptibility to intergranular corrosion and electrochemical reactivation behaviour of aisi 316l type stainless steel g. Duplex stainless steel welds and their susceptibility to. Bend test was used as a criterion to categorise the dos, which was then correlated to values of epr parameters and ec amplitude.
George corrosion igc by using various test s speci ed by. Plymouth offers our customers the industrys most current testing options and can even work with you on complex applications to determine exactly what testing should be required. Astm a262 practice a, b, c, e and f intergranular corrosion testing. Use of eddy current testing method in detection and evaluation of sensitisation and intergranular corrosion in austenitic stainless steels.
Detecting susceptibility to intergranular attack in austenitic stainless steels sections 8 to 14, inclusive, 1. Pdf assessment of intergranular corrosion in aisi type. The use of astm a262 practice a and e tests indicated sensitisation in base metal aged for 20 h and above. The weld zone of both the stainless steels suffered from cracking during astm a262 practice e, while the parent metals and hazs did not show such fissures. Astm a 763 sensitization testing of ferritic steels.
What is astm a262 intergranular corrosion test igc china. In hot strong nitric acid solutions, stainless steels exhibit intergranular corrosion. Nautic steels uk kobe, nssmc, sanyo japan posco korea schoeller bleckmann austria. Corrosion performance and fabricability of the new gen. Pdf use of eddy current testing method in detection and. Unitsthe values stated in inchpound units are to be regarded as standard. Mechanical testing metallurgical testing chemical analysis. Modified astm a262 standard practices ecoppercopper sulfate, sulfuric acid test for detecting susceptibility. The samemeasurements can be achieved using image analysis per practice e1245.
Astm a262 practice e strauss test this procedure is conducted to determine the susceptibility of austenitic stainless steel to inter granular attack associated with the precipitation of chromiumrich carbides. The first and fastest step is the astm a262 practice a, a rapid sameday screening method in oxalic acid to determine the susceptibility to intergranular corrosion. To date research has been conducted primarily on the parent material and heat affected zones in. For annual book of astm standards volume information, refer to the standards document summary page on the astm website. Note that practices a262 requires the test to be performed on sensitized specimens in the low. The manufacturer is not required to run the test unless it is specified on the purchase order see supplementary requirement s7. This test is used exclusively to determine corrosion in areas high in chromium carbide formations, and is. Strauss test astm a262 practice e this test is used exclusively to determine corrosion in areas high in chromium carbide formations, and is not as effective for intergranular attack caused by other means. Today, some,000 astm standards are used around the world to improve product quality, enhance safety, facilitate market access and trade. Access astm standards from any browser on your computer, tablet or smart phone. Exceeding your expectations with quality, service and delivery. Astm a262 practice e and electrochemical reactivation test method was shown by novak et al. The etch structure types used to classify the specimens are.
Standard practices for detecting susceptibility to intergranular attack. Use of eddy current testing method in detection and. As soon as the transaction is completed, your astm standards subscription will be ready for access. If two samples are polished for testing using one as a control sample. Us steel usa tubos spain vallourec tubes germany, france, brazil. There is no pdf download available at this time, however you may purchase a copy. Astm international by sections and volumes section 1. Corrosion performance and fabricability of the new generation of highly corrosionresistant. Astm a262 practice aoxalic acid etch test astm a262 practice bferric sulfatesulfuric acid test astm a262 practice cnitric acid test astm a262 practice ecoppercopper sulfatesulfuric acid test practical demonstration of testing of stainless steel material. In the table below, some results from this test are presented. Astma262 standard practices for detecting susceptibility to intergranular attack in austenitic stainless steels. The use of astm a262 practice a and e tests indicated sensitisation in.
One of the two samples is boiled in a copper copper sulfate sulfuric acid solution for a specified period of time while the other. The moneypennystrauss test heat treats the sample in the sensitizing temperature range in order to determine the materials resistance to intergranular corrosion. Modified astm a262 standard practices ecoppercopper sulfate sulfuric acid test for detecting susceptibility to intergranular attack was used. The astm a262 specification covers the standard practices for detecting susceptibility to intergranular attack in austenitic stainless steels. Assessment of intergranular corrosion in aisi type 316l stainless steel weldments. Determination of susceptibility to intergranular corrosion. Intergranular corrosion testing of austenitic stainless steels in.
Astm a262 intergranular corrosion testing and analysis. Astm international, formerly known as the american society for testing and materials astm, is a globally recognized leader in the development and delivery of international voluntary consensus standards. Astm a 262 test, intergranular corrosion, igc, astm a262 practice. This test is particularly useful in production control of exfoliation resistant heat treatments for the 2000, 5000, and 7000 series aluminum alloys. Every industry, application, and product has unique specification requirements including specialty testing and nde. A262 98 standard practices for detecting susceptibility to intergranular attack in austenitic stainless steels, austenitic steelstainless steel, copper sulfate, corrosion testing, etch structures, ferric sulfate, intergranular corrosion, nitric acid, oxalic acid.
Practice e exposure of aged stainless steel led to dissolution of the crdepleted regions. This practice covers the examination of tubular products ranging in diameter from 0. Alternate immersion corrosion testing per the astm g 44 standard practice. A262 14 standard practices for detecting susceptibility to intergranular attack in austenitic stainless steels, austenitic stainless steel, copper sulfate, corrosion testing, etch structures, ferric sulfate, intergranular corrosion, nitric acid, oxalic acid. A26214 standard practices for detecting susceptibility to.
Astm a262 15 standard practices for detecting susceptibility to. A similar trend of degree of sensitization was observed in the haz where it was higher in the 304ln1 as compared to the 304ln2. This specification covers the standard practices for detecting susceptibility to intergranular attack in austenitic stainless steels. A26214 standard practices for detecting susceptibility to intergranular attack in austenitic stainless steels, 2014 you currently cannot view this content. For comparison, 304l ss, which is currently used in reprocessing plants, was also studied. The specimen was covered with copper shot and grindings and immersed in a solution of 16 wt% sulfuric acid with 6 wt% copper sulfate.
Intergranular corrosion behavior of 304ln stainless steel. The nitric acidhydrofluoric acid test of a262, practice d, the acidified copper sulfate test of a708, and the 24hour copper accelerated, acidified copper sulfate test in a262, practice e, are also applicable to ati 20 alloy in the annealed and annealed plus sensitized condition. The higher alloyed materials 22, c2000, 59 and 686 have sufficient. Pdf assessment of intergranular corrosion in aisi type 316l. Astm a312 stainless steel tube shall be furnished in heat treatment condition comply to. G2mt labs metallurgy, corrosion, and failure analysis experts. All bsi british standards available online in electronic and print formats.
These practices include five intergranular corrosion tests, namely. Active standard astm a262 developed by subcommittee. Astm international, 100 barr harbor drive, po box c700, west conshohocken, pa, 194282959 usa. This means that there is very little risk of carbide precipitation during heating, for example when welding. Classification of the structure after a262 practice a analysis will determine if the material is acceptable or if additional testing is required. Astm a262, practice e is a common test for intergranular corrosion igc. Manufacturer of andstainless ornamental structural tubing. Corrosion testing techniques and evaluation practices used in industry.
1281 799 333 1498 185 206 884 228 268 646 131 1024 1544 35 228 1489 270 162 1521 1153 34 8 1206 1481 1075 970 805 31 1376 111 1453 752 661 725